Quality control of fiber counts
 

CQ Fibres
Since 1992, the IRSST has had a quality control program for fibre counting with samples originating from different Québec workplaces. According to the requirements of the official counting method, fibre counters must participate in an interlaboratory exchange program using samples that are representative of their industrial activities, thus allowing their efficiency to be verified. Every three months, the participating analysts receive four samples. After three successful consecutive exchanges, based on specific criteria, they receive a certificate confirming their efficiency. This remains in force as long as they participate in the program and meet these criteria. The list of recognized laboratories and counters is updated every three months.

Program description Important Dates
Classification criteria Care and shipment of quality control slides
Program registration Sending results
Fees For more information
  List of recognized counters and laboratories

Program description
Fiber counting will be done on mixed cellulose ester membranes mounted on slides in our laboratory and will come from sampling done in various Quebec workplaces.  The homogeneity of slides has been verified before their arrival to each participant. Samples must be counted in accordance with the IRSST 243-1 method - Free Download.

Each round will consist of a series of four test slides of various densities (<100 to 1300 f/mm²).  Each year, four rounds will be shipped to counters registered in the program to evaluate their performance and/or to obtain their recognition. Individual reports are mailed to participants at the conclusion of each round and, once recognized, the counter’s name will appear on the IRSST web site, at http://www.irsst.qc.ca/en/_compteurs.html.

Performance results will be sent to counters on an individual basis.  This report will include the following information:  counter's results, reference count, density ratios, the coefficient of variation and the upper and lower performance limits.  This is the manner in which you will be informed of your performance and progress in the program.  Performance is judged acceptable when at least 3 out of 4 results are within the performance limits (see "Classification criteria"). 


Classification criteria
The average count for these samples is established from the results of twelve experienced counters having already demonstrated their acceptable performances in various interlaboratory exchanges.

In order to be recognized, a counter must participate and succeed in 3 successive interlaboratory exchanges:

  • The counter's results must fall between 0,55 and 2,20 inclusively of the target value for at least three (3) samples out of four (4);
  • His status is maintained as long as he satisfies these requirements in subsequent rounds;
  • If two (2) or more results out of four (4) are not acceptable, an immediate loss of the counter's status would result. This will put him into a transition period. He may regain his status after having successfully completed two successive interlaboratory exchanges.

Program registration
With your registration form, you must supply a detailed description of the training you've received and the name, title and experience of the instructor. (A copy of an attestation or certificate from a recognized organization will suffice.)  Moreover, you must submit results obtained for three slides with different fiber densities counted ten times each, to determine  your intracounter relative standard deviation. (please use the Excel file to submit your results « Result-3X10.xls »).

A set of 4 slides will be shipped to each laboratory (to the contact person) four times a year.  The shipment will include a form to report results for each counter.  These forms must be completed and returned to the IRSST (accompanied by the slides) within one month after reception of the set.  (See  Table of important dates.)

If you add or change a registration during the year, please let us know.

Fees

LABORATORY

Initial registration

200 $

ANALYST(S)

Initial registration

50 $ per analyst

PARTICIPATION FEE

Annual laboratory fee

200 $

Cost for each participating analyst

100 $ per series 

  • Registration form (Download)  
  • Analyst form (Download)
  • Results file for intra-counter RSD determination (3 slides counted 10 times each) (Download)
     
    PAYMENT: An invoice will be mailed upon receipt of an application, or at the time of a modification (addition or removal of an analyst) and for the annual participating fee.
  • Important dates

    Important dates for 2010 rounds are presented in the following table:
     

    Serial number 

    2101

    2102

    2103

    2104

    Samples received

    02-12-2010

    05-14-2010

    08-13-2010

    11-12-2010

    Results
    received
    (IRSST)

    03-12-2010

    06-15-2010

    09-15-2010

    12-15-2010

    Reports mailed

     04-15-2010

    07-15-2010

    10-15-2010

    14-01-2011

    If you haven't received samples at the date in the first row, contact us quickly at (514) 288-1551 ext. 246.

    Results and samples (slides)* must be received by the date in the second row in order for your performance to be evaluated.  All results received after this date will be considered outliers and the counter will have failed the round.

    *Note: You are responsible for the safe shipment of slides to prevent breakage.


    Care and shipment of quality control slides

    All slides should be kept out of direct sunlight.

    When returning slides, we recommend the following procedure:

    • Slides are placed in their plastic box and then are shipped in a padded envelope to;
      • Mr Martin Beauparlant
        IRSST
        Research Department 
        505 De Maisonneuve West Blvd 
        12th floor
        Montréal (Québec) H3A 3C2

    Sending results
    We would like to inform all participants who chose to fax or e-mail results, that we need to receive the original, completed and signed form also.  Also, we must remind participants of the importance of returning the slides back to us by the deadline; your results will no longer be processed if the slides haven’t been returned on time.

    For more information
    Any questions concerning the fiber counting quality control program may be addressed to:

    Mr Martin Beauparlant
    IRSST
    Research Department  
    505 De Maisonneuve West Blvd
    Montréal, Québec
    H3A 3C2

    Telephone: (514) 288-1551 ext. 336
    Fax: (514) 288-9632
    E-mail: cqfibres@irsst.qc.ca

    OR

    Ms Claudette M. Dufresne

    Telephone: (514) 288-1551 ext. 405
    Fax : (514) 288-9632
    E-mail: cqfibres@irsst.qc.ca

    OR

    Ms Catheline Pelletier

    Telephone : (514) 288-1551 ext. 364 ou 246
    Fax: (514) 288-9632
    E-mail : cqfibres@irsst.qc.ca

     

    List of recognized counters and laboratories
    Participating labs in our quality control program have their recognized counters listed on our web site.  This list is updated at the conclusion of each round and lets you and your clients know how the fibre counters are performing.    http://www.irsst.qc.ca/en/_compteurs.html

     

     

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